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VASSANELLI LAB ANALYSES

METHYL ESTERS OF FATTY ACIDS

ANALYTICAL TECHNIQUE: GC-FID

UNIT OF MEASUREMENT: %

METHOD: Reg CEE 2568/1991 11/07/1991 GU CEE L248 05/09/1991 All X Reg UE 1833/2015 12/10/2015 GU UE L266/29 13/10/2015 All IV

MATRICES ( A if accredited) : Oil A

DESCRIPTION:

Package Code: PG00312

(for esters from C14 to C24 inclusive)

The method is suitable for the determination of:

- C14: 0 (Myristic Acid)

- C16: 0 (Palmitic Acid)

- C16: 1 (Palmitoleic Acid)

- C17: 0 (Heptadecanoic Acid)

- C17: 1 (Cis-10-Heptadecenoic Acid)

- C18: 0 (Stearic Acid)

- C18: 1n9c (Oleic Acid)

- C18: 2n6c (Linoleic Acid)

- C18: 3n3 (Alpha-Linolenic Acid)

- C20: 0 (Arachic Acid)

- C20: 1n9 (Cis-11-Eicosenoic Acid)

- C22: 0 (Behenic Acid)

- C24: 0 (Lignoceric Acid)

Updated accreditation of parameters: see accredia on-line link

The fatty acids of the glycerides present in the oil are transformed, via transesterification, into their respective methyl esters, which have greater volatility and lower polarity than the corresponding free acids. analytical determination of the methyl esters of the fatty acids makes it possible to obtain the percentage of individual chemical components present in an oil. The determination takes place via gc-fid (gas chromatography with flame photometric detector).

An acidic composition represents an indicator of the oil's authenticity and typical character.



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